HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexylamine → 2,5-Dimethylhexane-2,5-diyl bis(2-(hexylamino)acetate)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexylamine | HCID 8102 | — |
| Reactant | 2,5-Dimethylhexane-2,5-diyl bis(2-chloroacetate) | HCID 58282150 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2,5-Dimethylhexane-2,5-diyl bis(2-(hexylamino)acetate) | HCID 86653836 | — |
Reaction Steps
The cleavable diol is made by the following manner. Compound (61) is reacted with 5 equivalents of 1-aminohexane (65) in methylene chloride. Wash with brine and dry to yield 2,5-dimethylhexane-2,5-diyl bis(2-(hexylamino)acetate) (66).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08349990B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-59e398b68fba4a6c8498d77fe24e5e51 |
| Source note | uspto-grants-2013_01 |