HCID 66775446, compound → HCID 58807411, compound

HRID 1803647Notes

Reaction equation

HRID 1803647 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([F:15])[C:5]([CH:9]=[CH:10][C@H:11]([CH3:14])[CH2:12][CH3:13])=[C:6]([F:8])[CH:7]=1>CCCCCCC.[Pt]>[Br:1][C:2]1[CH:7]=[C:6]([F:8])[C:5]([CH2:9][CH2:10][C@H:11]([CH3:14])[CH2:12][CH3:13])=[C:4]([F:15])[CH:3]=1

Participants

4

Reactant 1

HCID 66775446HCID 66775446, compound

Product 1

HCID 58807411HCID 58807411, compound

Reagents, catalysts & solvents 2

HCID 23939PlatinumCatalystHCID 8900HeptaneSolvent

Procedure

0.4 g of 5% Pt/C (dry) is added to a solution of 1.8 g (5.9 mmol) of 2 in 50 ml of heptane, and the mixture is hydrogenated at atmospheric pressure for 20 hours. The solvent is removed under reduced pressure, and the entire amount is converted into 4.

Workup

  1. customThe solvent is removed under reduced pressure

Sources & evidence

ORD record
ord-c0c259702a9844af97d15c788d17492e
Source dataset
uspto-grants-2013_01
Patent number
US08350100B2

Reaction notes

Loading…