huagongshe.com
HRID1803933

反应详情

EQUATION

反应方程式

HRID 1803933 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(N2CCNCC2)c(C)c1
HCID70544

1-(2,4-Xylyl)piperazine

C12H18N2

结构：O=C(O)c1ccc(Br)c(Cl)c1
HCID12594302

4-Bromo-3-chlorobenzoic acid

C7H4BrClO2

PRODUCTS

生成物

1
结构：Cc1ccc(N2CCN(C(=O)c3ccc(Br)c(Cl)c3)CC2)c(C)c1
HCID58484864

未命名化合物

收率 100.7%

PROCEDURE

实验过程

By reaction and treatment in the same manner as in Preparation Example 1 and using 4-bromo-3-chlorobenzoic acid (2.4 g) and 1-(2,4-dimethylphenyl)piperazine (1.9 g), the title compound (4.1 g) was obtained.

WORKUP

后处理

  1. customBy reaction and treatment in the same manner
  2. customas in Preparation Example 1