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HRID1803971

反应详情

EQUATION

反应方程式

HRID 1803971 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)c1ccc(Br)cn1
HCID608544

5-bromopyridine-2-carboxylic acid

C6H4BrNO2

结构：Cl.O=C(c1ccc(Cl)cc1)C1CCNCC1
HCID2777114

(4-Chlorophenyl)(piperidin-4-yl)methanone--hydrogen chloride (1/1)

C12H15Cl2NO

PRODUCTS

生成物

1
结构：O=C(c1ccc(Cl)cc1)C1CCN(C(=O)c2ccc(Br)cn2)CC1
HCID58484577

未命名化合物

收率 99.1%

PROCEDURE

实验过程

By reaction and treatment in the same manner as in Preparation Example 27 and using 5-bromopyridine-2-carboxylic acid (1.2 g) and (4-chlorophenyl)piperidin-4-ylmethanone hydrochloride (1.6 g), the title compound (2.4 g) was obtained.

WORKUP

后处理

  1. customBy reaction and treatment in the same manner
  2. customas in Preparation Example 27