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HRID1804009

反应详情

EQUATION

反应方程式

HRID 1804009 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)c1ccc(Br)cc1[N+](=O)[O-]
HCID3774467

4-Bromo-2-nitrobenzoic acid

C7H4BrNO4

结构：Cc1cnc(N2CCNCC2)c(C)c1
HCID58484496

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cnc(N2CCN(C(=O)c3ccc(Br)cc3[N+](=O)[O-])CC2)c(C)c1
HCID58484547

未命名化合物

收率 90.3%

PROCEDURE

实验过程

By reaction and treatment in the same manner as in Preparation Example 60 and using 4-bromo-2-nitrobenzoic acid (2.3 g) and 1-(3,5-dimethylpyridin-2-yl)piperazine (1.91 g) described in Preparation Example 47, the title compound (3.54 g) was obtained.

WORKUP

后处理

  1. customBy reaction and treatment in the same manner
  2. customas in Preparation Example 60
  3. customdescribed in Preparation Example 47