HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Bromo-2-nitrobenzoic acid → (4-Bromo-2-nitrophenyl)[4-(3,5-dimethylpyridin-2-yl)piperazin-1-yl]methanone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Bromo-2-nitrobenzoic acid | HCID 3774467 | — |
| Edukt | 1-(3,5-Dimethylpyridin-2-yl)piperazine | HCID 58484496 | — |
| Produkt | (4-Bromo-2-nitrophenyl)[4-(3,5-dimethylpyridin-2-yl)piperazin-1-yl]methanone | HCID 58484547 | 90,3% |
Reaktionsschritte
By reaction and treatment in the same manner as in Preparation Example 60 and using 4-bromo-2-nitrobenzoic acid (2.3 g) and 1-(3,5-dimethylpyridin-2-yl)piperazine (1.91 g) described in Preparation Example 47, the title compound (3.54 g) was obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08354401B2 |
| Quelldatensatz | uspto-grants-2013_01 |
| ORD ID | ord-a797f5c141b04e10a6d89c0ec1526c1c |
| Quellennotiz | uspto-grants-2013_01 |