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HRID1804020

反应详情

EQUATION

反应方程式

HRID 1804020 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)c1ccc(Br)nc1
HCID238932

6-Bromonicotinic acid

C6H4BrNO2

结构：Cc1cnc(N2CCNCC2)c(C)c1
HCID58484496

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cnc(N2CCN(C(=O)c3ccc(Br)nc3)CC2)c(C)c1
HCID58484661

未命名化合物

收率 99.9%

PROCEDURE

实验过程

By reaction and treatment in the same manner as in Preparation Example 67 and using 6-bromonicotinic acid (808 mg) and 1-(3,5-dimethylpyridin-2-yl)piperazine (765 mg) described in Preparation Example 47, the title compound (1.5 g) was obtained.

WORKUP

后处理

  1. customBy reaction and treatment in the same manner
  2. customas in Preparation Example 67
  3. customdescribed in Preparation Example 47