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HRID1804036

反应详情

EQUATION

反应方程式

HRID 1804036 的结构方程式

REACTANTS

反应物

2
结构：CS(=O)(=O)c1cc(Br)ccc1C(=O)O
HCID2761057

4-Bromo-2-(methylsulfonyl)benzoic acid

C8H7BrO4S

结构：c1nc(N2CCNCC2)c(C2CC2)cc1C1CC1
HCID58484701

未命名化合物

PRODUCTS

生成物

1
结构：CS(=O)(=O)c1cc(Br)ccc1C(=O)N1CCN(c2ncc(C3CC3)cc2C2CC2)CC1
HCID58484601

未命名化合物

收率 73%

PROCEDURE

实验过程

By reaction and treatment in the same manner as in Preparation Example 38 and using 4-bromo-2-methanesulfonylbenzoic acid (2.29 g) and 1-(3,5-dicyclopropylpyridin-2-yl)piperazine (2 g) described in Preparation Example 62, the title compound (3.02 g) was obtained.

WORKUP

后处理

  1. customBy reaction and treatment in the same manner
  2. customas in Preparation Example 38
  3. customdescribed in Preparation Example 62