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HRID1804042

反应详情

EQUATION

反应方程式

HRID 1804042 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)c1ccc(I)cc1
HCID74373

Benzoyl chloride, 4-iodo-

C7H4ClIO

结构：c1nc(N2CCNCC2)c(C2CC2)cc1C1CC1
HCID58484701

未命名化合物

PRODUCTS

生成物

1
结构：O=C(c1ccc(I)cc1)N1CCN(c2ncc(C3CC3)cc2C2CC2)CC1
HCID58484688

未命名化合物

收率 90.9%

PROCEDURE

实验过程

By reaction and treatment in the same manner as in Preparation Example 65 and using 1-(3,5-dicyclopropylpyridin-2-yl)piperazine (5.52 g) described in Preparation Example 62, 4-iodobenzoyl chloride (6.35 g), the title compound (9.76 g) was obtained.

WORKUP

后处理

  1. customBy reaction and treatment in the same manner
  2. customas in Preparation Example 65