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HRID1804049

反应详情

EQUATION

反应方程式

HRID 1804049 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)c1ccc(Br)cc1F
HCID2734026

4-Bromo-2-fluorobenzoyl chloride

C7H3BrClFO

结构：CCc1cnc(N2CCNCC2)c(C)c1.Cl
HCID67380924

未命名化合物

PRODUCTS

生成物

1
结构：CCc1cnc(N2CCN(C(=O)c3ccc(Br)cc3F)CC2)c(C)c1
HCID58484537

未命名化合物

收率 99.2%

PROCEDURE

实验过程

By reaction and treatment in the same manner as in Preparation Example 8 and using 4-bromo-2-fluorobenzoyl chloride (2.4 g) and 1-(5-ethyl-3-methylpyridin-2-yl)piperazine hydrochloride (2.4 g) described in Preparation Example 99, the title compound (4 g) was obtained.

WORKUP

后处理

  1. customBy reaction and treatment in the same manner
  2. customas in Preparation Example 8
  3. customdescribed in Preparation Example 99