HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(5-Bromo-3-methylpyridin-2-yl)piperazine → HCID 58484740, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(5-Bromo-3-methylpyridin-2-yl)piperazine | HCID 46739270 | — |
| Reactant | 6-Fluoro-4-methylpyridine-3-carboxylic acid | HCID 46739274 | — |
| Product | HCID 58484740 | HCID 58484740 | 43.4% |
Reaction Steps
By reaction and treatment in the same manner as in Preparation Example 69 and using 6-fluoro-4-methylnicotinic acid (931 mg) and 1-(5-bromo-3-methylpyridin-2-yl)piperazine (1.5 g), the title compound (1 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08354401B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-125e8a21052c4df7ad44c96b6a00f346 |
| Source note | uspto-grants-2013_01 |