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HRID1804070

反应详情

EQUATION

反应方程式

HRID 1804070 的结构方程式

REACTANTS

反应物

2
结构：CS(=O)(=O)Nc1cc(Br)ccc1C(=O)O
HCID22621082

未命名化合物

结构：Cc1cnc(N2CCNCC2)c(C)c1
HCID58484496

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cnc(N2CCN(C(=O)c3ccc(Br)cc3NS(C)(=O)=O)CC2)c(C)c1
HCID58484868

未命名化合物

收率 21%

PROCEDURE

实验过程

By reaction and treatment in the same manner as in Preparation Example 60 and using 4-bromo-2-methanesulfonylaminobenzoic acid (0.964 g) described in Preparation Example 122 and 1-(3,5-dimethylpyridin-2-yl)piperazine (0.629 g) described in Preparation Example 47, the title compound (0.321 g) was obtained.

WORKUP

后处理

  1. customBy reaction and treatment in the same manner
  2. customas in Preparation Example 60
  3. customdescribed in Preparation Example 47