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HRID1804071

反应详情

EQUATION

反应方程式

HRID 1804071 的结构方程式

REACTANTS

反应物

2
结构：CS(=O)(=O)Nc1cc(Br)ccc1C(=O)O
HCID22621082

未命名化合物

结构：Cc1cc(C2CC2)cnc1N1CCNCC1
HCID58484718

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(C2CC2)cnc1N1CCN(C(=O)c2ccc(Br)cc2NS(C)(=O)=O)CC1
HCID58484826

未命名化合物

收率 79.9%

PROCEDURE

实验过程

By reaction and treatment in the same manner as in Preparation Example 60 and using 4-bromo-2-methanesulfonylaminobenzoic acid (1 g) described in Preparation Example 122 and 1-(5-cyclopropyl-3-methylpyridin-2-yl)piperazine (0.739 g) described in Preparation Example 96, the title compound (1.34 g) was obtained.

WORKUP

后处理

  1. customBy reaction and treatment in the same manner
  2. customas in Preparation Example 60
  3. customdescribed in Preparation Example 96