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HRID1804096

反应详情

EQUATION

反应方程式

HRID 1804096 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)c1ccc(Br)nc1
HCID238932

6-Bromonicotinic acid

C6H4BrNO2

结构：CCc1cnc(N2CCNCC2)c(C)c1
HCID58484578

未命名化合物

PRODUCTS

生成物

1
结构：CCc1cnc(N2CCN(C(=O)c3ccc(Br)nc3)CC2)c(C)c1
HCID58484652

未命名化合物

收率 55%

PROCEDURE

实验过程

By reaction and treatment in the same manner as in Preparation Example 27 and using 6-bromonicotinic acid (500 mg) and 1-(5-ethyl-3-methylpyridin-2-yl)piperazine (586 mg) described in Preparation Example 53, the title compound (530 mg) was obtained.

WORKUP

后处理

  1. customBy reaction and treatment in the same manner
  2. customas in Preparation Example 27
  3. customdescribed in Preparation Example 53