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HRID1804113

反应详情

EQUATION

反应方程式

HRID 1804113 的结构方程式

REACTANTS

反应物

2
结构：O=C1N[C@H](COC(=O)c2ccccc2)CO1
HCID16213752

未命名化合物

结构：CC(C)(C)OC(=O)N1CCN(C(=O)c2ccc(I)cc2)CC1
HCID44157877

Tert-butyl 4-(4-iodobenzoyl)piperazine-1-carboxylate

C16H21IN2O3

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CCN(C(=O)c2ccc(N3C(=O)OC[C@H]3COC(=O)c3ccccc3)cc2)CC1
HCID58484870

未命名化合物

收率 90.3%

PROCEDURE

实验过程

By reaction and treatment in the same manner as in Preparation Example 91 and using 4-(4-iodobenzoyl)piperazine-1-carboxylic acid tert-butyl ester (3.75 g) described in Preparation Example 161 and benzoic acid (R)-2-oxooxazolidin-4-ylmethyl ester (1.99 g), the title compound (4.14 g) was obtained.

WORKUP

后处理

  1. customBy reaction and treatment in the same manner
  2. customas in Preparation Example 91