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HRID1804116

反应详情

EQUATION

反应方程式

HRID 1804116 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)N1CCNCC1
HCID143452

tert-Butyl piperazine-1-carboxylate

C9H18N2O2

结构：CS(=O)(=O)c1cc(Br)ccc1C(=O)O
HCID2761057

4-Bromo-2-(methylsulfonyl)benzoic acid

C8H7BrO4S

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CCN(C(=O)c2ccc(Br)cc2S(C)(=O)=O)CC1
HCID58484680

未命名化合物

收率 94.2%

PROCEDURE

实验过程

By reaction and treatment in the same manner as in Preparation Example 90 and using 4-bromo-2-methanesulfonylbenzoic acid (10.2 g) and piperazine-1-carboxylic acid tert-butyl ester (7.49 g), the title compound (15.4 g) was obtained.

WORKUP

后处理

  1. customBy reaction and treatment in the same manner
  2. customas in Preparation Example 90