HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-methanesulfonylbenzoic acid → HCID 67381409, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-methanesulfonylbenzoic acid | HCID 2761057 | — |
| Reactant | HCID 67381125 | HCID 67381125 | — |
| Product | HCID 67381409 | HCID 67381409 | 73.2% |
Reaction Steps
By reaction and treatment in the same manner as in Preparation Example 67 and using (R)-1-(2,4-dimethylphenyl)-2-methylpiperazine (1.2 g) and 4-bromo-2-methanesulfonylbenzoic acid (1.7 g), (4-bromo-2-methanesulfonylphenyl)[(R)-4-(2,4-dimethylphenyl)-3-methylpiperazin-1-yl]methanone (2.0 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08354401B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-f12f195b3a9644d382482126993eabe5 |
| Source note | uspto-grants-2013_01 |