Hydrochloric Acid → HCID 68967848, compound

HRID 1804547Notes

Reaction equation

HRID 1804547 reaction equation
[O:1]=[C:2]1[N:6]([C:7]2[CH:8]=[C:9]([CH:19]=[CH:20][CH:21]=2)[CH2:10][NH:11]C(=O)OC(C)(C)C)[CH2:5][CH2:4][O:3]1.[ClH:22]>ClCCl>[ClH:22].[NH2:11][CH2:10][C:9]1[CH:8]=[C:7]([N:6]2[CH2:5][CH2:4][O:3][C:2]2=[O:1])[CH:21]=[CH:20][CH:19]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 57698624HCID 57698624, compound

Product 1

HCID 68967848HCID 68967848, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

380 mg (1.30 mmol) tert-butyl [3-(2-oxo-oxazolidin-3-yl)-benzyl]-carbamate are placed in 2 ml dichloromethane, 4.00 ml (8 mmol) 2 molar ethereal hydrochloric acid are added. The mixture is stirred for 16 hours at ambient temperature, then evaporated down. The residue is lyophilised.

Workup

  1. customevaporated down

Sources & evidence

ORD record
ord-6f3fc64086294ee1a9b589c317efbcce
Source dataset
uspto-grants-2013_01
Patent number
US08354418B2

Reaction notes

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