HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-2-butanone → HCID 68905741, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-2-butanone | HCID 13156 | — |
| Reactant | tert-butyl N-(2-carbamothioylethyl)carbamate | HCID 2735653 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68905741 | HCID 68905741 | — |
Reaction Steps
2.00 g (9.50 mmol) tert.butyl N(3-amino-3-thioxopropyl)carbamate and 1.58 g (10.45 mmol) 1-bromo-2-butanone are refluxed in 40 ml of ethanol for 16 hours with stirring. The reaction mixture is evaporated down, the residue is purified by chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08354418B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-a9189c79f8924629af8c20cb301cbc8c |
| Source note | uspto-grants-2013_01 |