HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl [2-(5-ethyloxazol-2-yl)ethyl]carbamate → 2-(5-Ethyloxazol-2-yl)ethylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl [2-(5-ethyloxazol-2-yl)ethyl]carbamate | HCID 57636953 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-(5-Ethyloxazol-2-yl)ethylamine | HCID 11542801 | — |
Reaction Steps
2.86 g (10.43 mmol) benzyl [2-(5-ethyl-oxazol-2-yl)-ethyl]-carbamate are placed in 130 ml of methanol, 0.910 mg palladium/charcoal 10% are added, then the mixture is hydrogenated for 5 hours at ambient temperature under a pressure of 14 psi. Then the catalyst is suction filtered and the solution is evaporated down.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08354418B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-0bb8f8b4496347e4a8a9fb4994d8c8a2 |
| Source note | uspto-grants-2013_01 |