HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 24254482, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 57636978 | HCID 57636978 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 24254482 | HCID 24254482 | — |
Reaction Steps
2.95 g (12.23 mmol) tert-butyl [2-(5-ethyl-[1,3,4]oxadiazol-2-yl)-ethyl]-carbamate and 10 ml trifluoroacetic acid are stirred in 100 ml dichloromethane for 24 hours at ambient temperature. Then the mixture is evaporated down, the residue is made basic and extracted with ethyl acetate. The organic phase is dried and evaporated to dryness.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08354418B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-676548987f224d0baf44f630521d62b1 |
| Source note | uspto-grants-2013_01 |