HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18538721, compound → 956075-57-3
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18538721 | HCID 18538721 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 956075-57-3 | HCID 28063741 | 95% |
Reaction Steps
The title compound from Step B above (100 mg, 0.4 mmol) was dissolved in 4 M HCl in dioxane (4.0 mL) and stirred at RT for 1 h. The product was concentrated under reduced pressure and dried under high vacuum to give the title compound (i-28) (59 mg, 95%). ESI-MS calculated for C9H15N3: Exact Mass: 165.13. Found 166.12.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08354403B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-d4978eadc86c46b2a59b06ce4046329c |
| Source note | uspto-grants-2013_01 |