HCID 18538721, compound → 956075-57-3

HRID 1804595Notes

Reaction equation

HRID 1804595 reaction equation
[N:1]1([CH2:6][CH:7]2[CH2:12][CH2:11][N:10](C(OC(C)(C)C)=O)[CH2:9][CH2:8]2)[CH:5]=[CH:4][CH:3]=[N:2]1>Cl.O1CCOCC1>[N:1]1([CH2:6][CH:7]2[CH2:8][CH2:9][NH:10][CH2:11][CH2:12]2)[CH:5]=[CH:4][CH:3]=[N:2]1

Participants

4

Reactant 1

HCID 18538721HCID 18538721, compound

Product 1

HCID 28063741956075-57-3Yield 95%

Reagents, catalysts & solvents 2

HCID 313Hydrochloric AcidSolventHCID 312751,4-DioxaneSolvent

Procedure

The title compound from Step B above (100 mg, 0.4 mmol) was dissolved in 4 M HCl in dioxane (4.0 mL) and stirred at RT for 1 h. The product was concentrated under reduced pressure and dried under high vacuum to give the title compound (i-28) (59 mg, 95%). ESI-MS calculated for C9H15N3: Exact Mass: 165.13. Found 166.12.

Workup

  1. concentrationThe product was concentrated under reduced pressure
  2. customdried under high vacuum

Sources & evidence

ORD record
ord-d4978eadc86c46b2a59b06ce4046329c
Source dataset
uspto-grants-2013_01
Patent number
US08354403B2

Reaction notes

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