HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67972218, compound → HCID 67060710, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67972218 | HCID 67972218 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 67060710 | HCID 67060710 | — |
Reaction Steps
The title compound from Step B above (200 mg, 0.68 mmol) was dissolved in 4 M HCl in dioxane (4.0 mL) and stirred at RT for 1 h. The product was concentrated under reduced pressure and dried under high vacuum to the title compound (i-37) (127 mg, 96%). ESI-MS calculated for C9H15N5: Exact Mass: 193.13. Found 194.14.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08354403B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-0295ce42d1b84493a23b3862506c7628 |
| Source note | uspto-grants-2013_01 |