HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 178435594, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178504179 | HCID 178504179 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178435594 | HCID 178435594 | — |
Reaction Steps
To a stirring solution of compound (S)-2-(5-trimethylsilanylethynyl-1H-benzoimidazol-2-yl)-piperidine-1-carboxylic acid benzyl ester (85.3 mg, 0.197 mmol) in MeOH (2 mL) is added potassium carbonate (27.3 mg, 0.197 mmol). The reaction mixture is stirred at room temperature for 3 hours and concentrated in vacuum to dryness. The residue obtained is used directly in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08354419B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-c40735aef6aa4674843a10cd705f61d8 |
| Source note | uspto-grants-2013_01 |