HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67151586, compound → HCID 67151667, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67151586 | HCID 67151586 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67151667 | HCID 67151667 | — |
Reaction Steps
6-Methoxy-2-vinyl-pyrimidine-4-carboxylic acid methyl ester (130 mg) was combined with MeOH (5 ml) to give a light yellow solution. Pd/C 10% (13 mg) was added and the reaction mixture was hydrogenated with a balloon at RT for 4 hours. The reaction mixture was filtered and the filtrate was concentrated in vacuo to give title compound as an off white solid. MS (ISP) 197.1 ([M+H]
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08354441B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-4a5322c5edf244cea92956905fbaed77 |
| Source note | uspto-grants-2013_01 |