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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1805248Generated: November 1, 2026

HCID 67151586, compound → HCID 67151667, compound

https://huagongshe.com/reaction/1805248

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67151586HCID 67151586—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 67151667HCID 67151667—

Reaction Steps

6-Methoxy-2-vinyl-pyrimidine-4-carboxylic acid methyl ester (130 mg) was combined with MeOH (5 ml) to give a light yellow solution. Pd/C 10% (13 mg) was added and the reaction mixture was hydrogenated with a balloon at RT for 4 hours. The reaction mixture was filtered and the filtrate was concentrated in vacuo to give title compound as an off white solid. MS (ISP) 197.1 ([M+H]

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08354441B2
Source datasetuspto-grants-2013_01
ORD IDord-4a5322c5edf244cea92956905fbaed77
Source noteuspto-grants-2013_01