HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methylbutanal → HCID 178446418, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methylbutanal | HCID 11552 | — |
| Reactant | Glycine tert-butyl ester | HCID 151417 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178446418 | HCID 178446418 | 98.3% |
Reaction Steps
In a manner similar to the method described in Example 1a, glycine tert-butyl ester (0.65 g, 5 mmol) was reacted with isovaleraldehyde (Alfa) (0.43 g, 5 mmol) in CH2Cl2 at room temperature for 18 h to give [3-methyl-but-(E)-ylideneamino]-acetic acid tert-butyl ester as a colorless oil (0.98 g, 98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08354444B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-61d360f4058548b6838b8c48fc986e4b |
| Source note | uspto-grants-2013_01 |