Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1806719Generated: November 1, 2026

3-Chlorobenzaldehyde → HCID 178451237, compound

https://huagongshe.com/reaction/1806719

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-ChlorobenzaldehydeHCID 11477—
ReactantGlycine tert-butyl esterHCID 151417—
SolventDichloromethaneHCID 6344—
ProductHCID 178451237HCID 17845123795%

Reaction Steps

In a manner similar to the method described in Example 1a, glycine tert-butyl ester (1.31 g, 10 mmol) was reacted with 3-chlorobenzaldehyde (Aldrich) (1.4 g, 10 mmol) in CH2Cl2 at room temperature for 18 h to give {[1-(3-chloro-phenyl)-meth-(E)-ylidene]-amino}-acetic acid tert-butyl ester as a pale yellow oil (2.4 g, 95%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08354444B2
Source datasetuspto-grants-2013_01
ORD IDord-3a1a1b9329a54784af2826eccd142208
Source noteuspto-grants-2013_01