HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pivalaldehyde → HCID 178446417, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pivalaldehyde | HCID 12417 | — |
| Reactant | Glycine tert-butyl ester | HCID 151417 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178446417 | HCID 178446417 | 100.4% |
Reaction Steps
In a manner similar to the method described in Example 1a, glycine tert-butyl ester (0.65 g, 5 mmol) was reacted with trimethylacetaldehyde (Aldrich) (0.42 g, 5 mmol) in CH2Cl2 at room temperature for 20 h to give [2,2-dimethyl-prop-(E)-ylideneamino]-acetic acid tert-butyl ester as a colorless oil (1.0 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08354444B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-b8edee8a460a4e099e184054d86c4937 |
| Source note | uspto-grants-2013_01 |