HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycine tert-butyl ester → HCID 178451250, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycine tert-butyl ester | HCID 151417 | — |
| Reactant | 3-Cyclopropyl-3-methylbutanal | HCID 86640372 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178451250 | HCID 178451250 | 75.2% |
Reaction Steps
Step E In a manner similar to the method described in Example 1a, glycine tert-butyl ester (0.65 g, 5 mmol) was reacted with 3-cyclopropyl-3-methyl-butyraldehyde (0.68 g, 5.3 mmol) in CH2Cl2 at room temperature for 5 h to give [3-cyclopropyl-3-methyl-but-(E)-ylideneamino]-acetic acid tert-butyl ester as a colorless oil (0.9 g, 75%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08354444B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-9da494f0bd394f649ac9e42c88b302a0 |
| Source note | uspto-grants-2013_01 |