HuagongsheHuagongshe Chemistry Print Report · For research reference only
D-Psicose → 4-(4H-1,2,4-triazol-3-yl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | D-Psicose | HCID 441036 | — |
| Reactant | 6219-52-9 | HCID 2825224 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 4-(4H-1,2,4-triazol-3-yl)aniline | HCID 3052732 | — |
Reaction Steps
5-(4-Nitro-phenyl)-1H-[1,2,4]triazole (510 mg) was suspended in 50 mL of ethyl acetate and 56 mg of 10% Pd/C was added. The mixture was hydrogenated under 50 Psi for 100 min. The mixture was filtered and the filtrate was concentrate to give a solid. 497 mg
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08354444B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-e229335c2e8c4acab06ff3ec9c8d26d4 |
| Source note | uspto-grants-2013_01 |