HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59276872, compound → HCID 59277199, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59276872 | HCID 59276872 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 59277199 | HCID 59277199 | — |
Reaction Steps
170 mg 1-(1-methyl-1H-imidazol-2-yl)-5-nitro-2,3-dihydro-1H-indole are dissolved in 20 ml of tetrahydrofuran. To this are added 20 mg palladium on charcoal (10%) and the mixture is hydrogenated for 1 hour at ambient temperature. Then the catalyst is filtered off and the solvent is eliminated in vacuo. The crude product is extracted from diethyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08357689B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-78ed9dc2d34f41dbb9b772d263595b75 |
| Source note | uspto-grants-2013_01 |