HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1807435Generated: October 30, 2026
HCID 178467949, compound → HCID 59277341, compound
https://huagongshe.com/reaction/1807435
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 178467949 | HCID 178467949 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 59277341 | HCID 59277341 | — |
Reaction Steps
470 mg N-(2,2-diethoxy-ethyl)-5-nitro-2,3-dihydro-indole-1-carboxamidine are dissolved in 8 ml trifluoroacetic acid and the mixture is heated to 60° C. for 3 hours. Then the solvent is eliminated in vacuo and the residue is chromatographed on aluminium oxide (dichloromethane/methanol 99:1 to 70:30).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08357689B2 |
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| Source dataset | uspto-grants-2013_01 |
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| ORD ID | ord-ea5e7ea682124fc5890c22b0468bac5b |
|---|
| Source note | uspto-grants-2013_01 |
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