HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 57420321, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 58092771 | HCID 58092771 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57420321 | HCID 57420321 | — |
Reaction Steps
A mixture of (3R,7aR)-7a-methoxymethyl-3-trichloromethyl-tetrahydro-pyrrolo[1,2-c]oxazol-1-one (Stage G.1, 0.6 g) and 7 M ammonia in MeOH (6 mL) was stood at rt for 2 days in a sealed vessel. The RM was then evaporated to give the title compound as a pale yellow oil which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08357707B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-bb21e97be27d41ec8a2dcf7d3b649778 |
| Source note | uspto-grants-2013_01 |