HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 57417082, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 58092718 | HCID 58092718 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57417082 | HCID 57417082 | — |
Reaction Steps
A solution of (2S,4S)-4-dimethylamino-pyrrolidine-2-carboxylic acid butyl ester (Stage Q.1, 326 mg) and 7 M ammonia in MeOH (8 ml) was stood for 18 h at it in a sealed vessel. Filtration, evaporation and trituration with Et2O/MeOH gave the title compound as a beige solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08357707B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-f46b9aa8b934416aba7cc6d2392125d6 |
| Source note | uspto-grants-2013_01 |