HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 86649530, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 58092750 | HCID 58092750 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86649530 | HCID 86649530 | — |
Reaction Steps
7-tert-Butyl-4,5-dihydro-benzo[1,2-d;3,4-d′]bisthiazol-2-ylamine (Stage T.1, 175 mg, 0.659 mmol) was dissolved in DCM (10 mL), CDI (297 mg, 1.648 mmol) was then added, and the RM was stirred at rt for 2 h. The title compound was isolated by filtration, washed with DCM and dried under HV.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08357707B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-a89f3efb50a844c9b4891e2888af7d4a |
| Source note | uspto-grants-2013_01 |