1,1'-Carbonyldiimidazole → HCID 86649530, compound

HRID 1807672Notes

Reaction equation

HRID 1807672 reaction equation
[C:1]([C:5]1[S:6][C:7]2[CH2:17][CH2:16][C:11]3[N:12]=[C:13]([NH2:15])[S:14][C:10]=3[C:8]=2[N:9]=1)([CH3:4])([CH3:3])[CH3:2].[CH:18]1[N:22]=[CH:21][N:20]([C:23](N2C=NC=C2)=[O:24])[CH:19]=1>C(Cl)Cl>[C:1]([C:5]1[S:6][C:7]2[CH2:17][CH2:16][C:11]3[N:12]=[C:13]([NH:15][C:23]([N:20]4[CH:19]=[CH:18][N:22]=[CH:21]4)=[O:24])[S:14][C:10]=3[C:8]=2[N:9]=1)([CH3:4])([CH3:2])[CH3:3]

Participants

4

Reactant 2

HCID 682631,1'-CarbonyldiimidazoleHCID 58092750HCID 58092750, compound

Product 1

HCID 86649530HCID 86649530, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

7-tert-Butyl-4,5-dihydro-benzo[1,2-d;3,4-d′]bisthiazol-2-ylamine (Stage T.1, 175 mg, 0.659 mmol) was dissolved in DCM (10 mL), CDI (297 mg, 1.648 mmol) was then added, and the RM was stirred at rt for 2 h. The title compound was isolated by filtration, washed with DCM and dried under HV.

Sources & evidence

ORD record
ord-a89f3efb50a844c9b4891e2888af7d4a
Source dataset
uspto-grants-2013_01
Patent number
US08357707B2

Reaction notes

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