HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68509556, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methyl 2-benzylisoindoline-5-carboxylate | HCID 23301778 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68509556 | HCID 68509556 | — |
Reaction Steps
HCl gas was passed through a solution of methyl 2-benzylisoindoline-5-carboxylate (56 g; 1 equiv.) in 560 ml of dichloromethane until a solid formed. The solid was filtered out, washed with hexane and dried. Methyl 2-benzylisoindoline-5-carboxylate hydrochloride (43 g) was obtained in the form of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08357717B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-d5ed4785bd2e4d158c67517f8a6654dc |
| Source note | uspto-grants-2013_01 |