HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → 2-Ethylhexanoic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | N-vinyl-2-pyrrolidone | HCID 6917 | — |
| Reactant | 2-Ethylhexyl acrylate | HCID 7636 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-Ethylhexanoic Acid | HCID 8697 | — |
Reaction Steps
Under an inert gas atmosphere, 72 parts by weight of 2-ethylhexyl acrylate, 25 parts by weight of N-vinyl-2-pyrrolidone, 3 parts by weight of acrylic acid, and 0.2 part by weight of azobisisobutyronitrile were added to ethyl acetate, and then the contents were mixed. The mixture was subjected to solution polymerization at 60° C. Thus, a solution (solid content: 28 w t %) of an acrylic copolymer (2-EHA/AA/N-VP=72/3/25) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08361493B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-0e9f5755bc1845dbabf1d01e321474c9 |
| Source note | uspto-grants-2013_01 |