HRID1808668

反应详情

EQUATION

反应方程式

HRID 1808668 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Eprosartan acetate (10 gm, obtained in example 1) is suspended in water (50 ml) at 25-30° C. and the pH of the suspension is adjusted to 7.0-7.25 with 5% sodium hydroxide solution (23 ml). The material is filtered, washed with water (20 ml) and then dried to give 8 gm of pure eprosartan free base (HPLC Purity: 99.85%).

WORKUP

后处理

  1. filtrationThe material is filtered
  2. washwashed with water (20 ml)
  3. customdried