HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59587918, compound → HCID 44595148, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59587918 | HCID 59587918 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 44595148 | HCID 44595148 | 47.9% |
Reaction Steps
Example 54 can be prepared in the same manner as example 46 from (3S,4S)-tert-butyl 3-azido-4-(but-2-ynyloxy)pyrrolidine-1-carboxylate (115 mg, 0.41 mmol) and xylene (10 ml), afforded the titled compound (55 mg, 47%) as white solid. M.p. 195-196° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08362011B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-8e37d398e3fd412c9ecd9ba4eddb8839 |
| Source note | uspto-grants-2013_01 |