HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59587968, compound → HCID 44595150, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59587968 | HCID 59587968 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 44595150 | HCID 44595150 | 88.2% |
Reaction Steps
Example 56 can be prepared in the same manner as example 53 from (3S,4S)-tert-butyl 3-azido-4-(3-(3-fluorophenyl)prop-2-ynyloxy)pyrrolidine-1-carboxylate (143 mg, 0.39 mmol) and toluene (12 ml), afforded the titled compound (124 mg, 86%) as white solid. M.p. 249-250° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08362011B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-505716592ddd4df89eae5181fc7c358c |
| Source note | uspto-grants-2013_01 |