HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 86652457, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 2,3-Dichloropyridine | HCID 16988 | — |
| Reactant | 2-Chloro-3-(trifluoromethyl)pyridine | HCID 589833 | — |
| Reactant | HCID 67094559 | HCID 67094559 | — |
| Product | HCID 86652457 | HCID 86652457 | 91% |
Reaction Steps
The procedure of Example 6 was repeated except for using 8-(6-(trifloromethyl)-1H-benzo[d]imidazol-2-yl)-3,4-dihydro-2H-benzo[b][1,4]oxazine and 2-chloro-3-trifluoromethylpyridine instead of 445-tert-butyl-1H-benzo[d]imidazol-2-yl)benzenamine and 2,3-dichloropyridine in Example 6 respectively to obtain the title compound (4.2 g, yield: 91%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08362012B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-b949c420eed446c6b7794103814ff1a3 |
| Source note | uspto-grants-2013_01 |