Hydrazine hydrate (1:1) → HCID 59322261, compound

HRID 1809251Notes

Reaction equation

HRID 1809251 reaction equation
Cl[C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[CH3:11])=[C:4]([NH:12][C:13]2[CH:20]=[CH:19][C:16]([C:17]#[N:18])=[CH:15][CH:14]=2)[N:3]=1.O.[NH2:22][NH2:23]>>[NH:22]([C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[CH3:11])=[C:4]([NH:12][C:13]2[CH:20]=[CH:19][C:16]([C:17]#[N:18])=[CH:15][CH:14]=2)[N:3]=1)[NH2:23]

Participants

3

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 59322243HCID 59322243, compound

Product 1

HCID 59322261HCID 59322261, compound

Procedure

Was prepared according to Example 8 from 4-(2-chloro-9-methyl-9H-purin-6-ylamino)-benzonitrile and hydrazine monohydrate.

Workup

  1. customWas prepared

Sources & evidence

ORD record
ord-7911ed7108824b0481fbbf9a076e623d
Source dataset
uspto-grants-2013_01
Patent number
US08362024B2

Reaction notes

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