Hydrazine hydrate (1:1) → HCID 59322256, compound
Reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9]2[N:17]=[C:16](Cl)[N:15]=[C:14]3[C:10]=2[N:11]=[CH:12][N:13]3[CH3:19])=[CH:4][CH:3]=1.O.[NH2:21][NH2:22]>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9]2[N:17]=[C:16]([NH:21][NH2:22])[N:15]=[C:14]3[C:10]=2[N:11]=[CH:12][N:13]3[CH3:19])=[CH:4][CH:3]=1Participants
3
Procedure
Was prepared according to Example 8 from (4-bromo-phenyl)-(2-chloro-9-methyl-9H-purin-6-yl)-amine and hydrazine monohydrate.
Workup
- customWas prepared
Sources & evidence
- ORD record
- ord-f71273f74dc04aad92d33988df446908
- Source dataset
- uspto-grants-2013_01
- Patent number
- US08362024B2
Reaction notes
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