HRID1809827

反应详情

EQUATION

反应方程式

HRID 1809827 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A palladium-carbon catalyst was added to a solution of 3-(3-fluoro-5-nitrophenoxy)pyridine (8.0 g) in methanol (70 ml), and the reaction solution was stirred under hydrogen atmosphere at room temperature for 2 hours. The reaction solution was filtered through Celite, and the filtrate was distilled off under reduced pressure to obtain a crude product as a yellow oil.

WORKUP

后处理

  1. filtrationThe reaction solution was filtered through Celite
  2. distillationthe filtrate was distilled off under reduced pressure