HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenacyl bromide → HCID 178462470, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenacyl bromide | HCID 6259 | — |
| Reactant | HCID 726326 | HCID 726326 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178462470 | HCID 178462470 | — |
Reaction Steps
A solution of methyl 4-(3-ethylthioureido)benzoate (2-3) (50 mg, 0.19 mmol) and 2-bromoacetophenone (39.8 mg, 0.20 mmol) in MeOH (1 mL) is heated to 80° C. for 2 hours and then cooled to room temperature and concentrated to provide (Z)-methyl 4-(3-ethyl-4-phenylthiazol-2(3H)-ylideneamino)benzoate (2-4).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08362050B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-9dd8e575ba974c6893ed5344b6d5fd97 |
| Source note | uspto-grants-2013_01 |