Hydrochloric Acid → HCID 68869432, compound

HRID 1809967Notes

Reaction equation

HRID 1809967 reaction equation
[ClH:1].[C:2]([CH2:4][C:5]1[O:9][C:8]([C:10]([O:12][CH2:13][CH3:14])=[O:11])=[CH:7][CH:6]=1)#[N:3].[CH2:15]([SH:22])[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>C(OCC)C>[ClH:1].[CH2:15]([S:22][C:2]([CH2:4][C:5]1[O:9][C:8]([C:10]([O:12][CH2:13][CH3:14])=[O:11])=[CH:7][CH:6]=1)=[NH:3])[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 7509Benzyl mercaptanHCID 39354641HCID 39354641, compound

Product 1

HCID 68869432HCID 68869432, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

Gaseous hydrogen chloride is passed for 30 minutes at 10° C. through a solution of 94.5 g (0.53 M) of ethyl 5-cyanomethylfuran-2-carboxylate and 61.9 ml (0.53 M) of benzyl mercaptan in 2000 ml of diethyl ether.

Sources & evidence

ORD record
ord-4eb655afd2644ab2bdf4b65c7eeffe8d
Source dataset
uspto-grants-2013_01
Patent number
US08362057B2

Reaction notes

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