HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 58149300, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | 2-(3-Bromo-5-chlorophenyl)acetic acid | HCID 15365222 | — |
| Product | HCID 58149300 | HCID 58149300 | — |
Reaction Steps
(3-Bromo-5-chloro-phenyl)-acetic acid (14 g, 56 mmol) in EtOH (150 mL) was treated with sulfuric acid (2 mL) at 50° C. for 2 hours. The mixture was worked-up with CH2Cl2 and H2O, and the organic layer was concentrated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08362044B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-3e8efc02cf1b4409a2e8eb525988b8d1 |
| Source note | uspto-grants-2013_01 |