Potassium Carbonate → HCID 11311797, compound

HRID 1810918Notes

Reaction equation

HRID 1810918 reaction equation
[CH2:1]([O:3][C:4](=[O:23])[C:5]1[CH:10]=[CH:9][C:8]([O:11][CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[C:7]([O:19]C(=O)C)[CH:6]=1)[CH3:2].C(=O)([O-])[O-].[K+].[K+]>CO>[CH2:1]([O:3][C:4](=[O:23])[C:5]1[CH:10]=[CH:9][C:8]([O:11][CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[C:7]([OH:19])[CH:6]=1)[CH3:2]

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 67170201HCID 67170201, compound

Product 1

HCID 11311797HCID 11311797, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The compound of step 1 (10 g, 31.8 mmol) was dissolved in methanol, potassium carbonate (88 mg, 0.636 mmol) was added and the mixture was stirred for 2 h under reflux. After evaporation to dryness, the residue was used without further purification in the subsequent step.

Workup

  1. temperatureunder reflux
  2. customAfter evaporation to dryness
  3. customthe residue was used without further purification in the subsequent step

Sources & evidence

ORD record
ord-847ccc0412f24323a43d8dcb4df6878b
Source dataset
uspto-grants-2013_01
Patent number
US08362073B2

Reaction notes

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